This method enables also oxidative lactonizations of unsaturated carboxylic acids in good to high yields. A clean and efficient and metal-free diacetoxylation reaction of alkenes using commercially available peroxyacids as the oxidants is catalyzed by triflic acid.

Y.-B.

Chemical yields range from 4% to 50%, the more basic thiazoles producing higher yields. Anhydrous [2-percarboxyethyl] functionalized silica is an advantageous oxidant for epoxidation of olefins. Kang, L. H. Gade, J. Org. The acidic silica surface does not catalyze ring-opening reactions except for particularly activated styrene oxide.

The oxidation of thiazoles by peroxy acids leads to the corresponding N -oxides.

Peroxy acids usually are prepared by reaction of the oxy acid with hydrogen peroxide; small amounts of sulfuric or other strong acids often are used to accelerate the reaction of weak oxy acids. Peracetic, m -chloroperbenzoic, permaleic, and trifluoroperacetic acid have been employed for this reaction. Chem., 2012, 77, 1610-1615. This organic peroxide is a colorless liquid with a characteristic acrid odor reminiscent of acetic acid… Alkenes carrying hydroxyl groups react with silica-supported peracid faster than unsubstituted alkenes. Peracetic acid is a component of antimicrobial washes for poultry carcasses and fruit. Peracetic acid (also known as peroxyacetic acid, or PAA), is a organic compound with the formula CH3CO3H.

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